Electropolymerisation of pyrrole onto aluminium from alkaline solutions containing a surfactant

Polypyrrole films have been successfully electrodeposited on aluminium substrates from alkaline solutions containing an anionic surfactant (sodium dodecyl sulphate or sodium dodecylbenzene sulfonate). Homogeneous and adherent films were formed under potentiostatic, galvanostatic and potentiodynamic...

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Detalles Bibliográficos
Autores: Saidman, Silvana Beatriz, Vela, Maria Elena
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2005
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/97813
Acceso en línea:http://hdl.handle.net/11336/97813
Access Level:acceso abierto
Palabra clave:ALUMINIUM
ELECTROPOLYMERISATION
POLYPYRROLE
SURFACTANT
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
Descripción
Sumario:Polypyrrole films have been successfully electrodeposited on aluminium substrates from alkaline solutions containing an anionic surfactant (sodium dodecyl sulphate or sodium dodecylbenzene sulfonate). Homogeneous and adherent films were formed under potentiostatic, galvanostatic and potentiodynamic control. The electrochemical response was compared to that obtained with vitreous carbon as a substrate. Studies performed in monomer-free solutions showed that both OH- and Na+ play an important role in the redox process. Scanning electron microscopy and atomic force microscopy studies indicated that the presence of surfactants influences the morphology of the polymer producing more homogeneous and less rough films than those formed in absence of surfactants.