Preparation and characterization of stainless steel 316L/HA biocomposite

The austenitic stainless steel 316L is the most used metallic biomaterials in orthopedics applications, especially in the manufacture of articulated prostheses and as structural elements in fracture fixation, since it has high mechanical strength. However, because it is biologically inactive, it doe...

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Bibliographic Details
Authors: Silva, Gilbert, Baldissera, Márcia Regina, Trichês, Eliandra de Sousa [UNIFESP], Cardoso, Kátia Regina [UNIFESP]
Format: article
Status:Published version
Publication Date:2013
Country:Brasil
Institution:Universidade Federal de São Paulo (UNIFESP)
Repository:Repositório Institucional da UNIFESP
Language:English
OAI Identifier:oai:repositorio.unifesp.br:11600/7725
Online Access:http://dx.doi.org/10.1590/S1516-14392012005000182
http://repositorio.unifesp.br/handle/11600/7725
Access Level:Open access
Keyword:biocomposite
stainless steels 316L
hydroxyapatite
mechanical alloying
Description
Summary:The austenitic stainless steel 316L is the most used metallic biomaterials in orthopedics applications, especially in the manufacture of articulated prostheses and as structural elements in fracture fixation, since it has high mechanical strength. However, because it is biologically inactive, it does not form chemical bond with bone tissue, it is fixed only by morphology. The development of biocomposites of stainless steel with a bioactive material, such as hydroxyapatite - HA, is presented as an alternative to improve the response in the tissue-implant interface. However significant reductions in mechanical properties of the biocomposite can occur. Different compositions of the biocomposite stainless steel 316L/HA (5, 20 and 50 wt. (%) HA) were prepared by mechanical alloying. After milling the powders for 10 hours, the different compositions of the biocomposite were compacted isostatically and sintered at 1200 ºC for 2 hours. The mechanical properties of the biocomposites were analyzed by compression tests. The powders and the sintered composites were analyzed by scanning electron microscopy (SEM) and X-ray diffraction (XRD).