Processing of the Nd2O3:SiO2 system by Laser Floating Zone in air
Highly textured polycrystalline fibres of monoclinic P21/c Nd2SiO5 and hexagonal P63/m Nd9.33(SiO4)6O2 phases were obtained by Laser Floating Zone in air from stoichiometric mixtures of Nd2O3 and SiO2 changing the pulling rate from 10 to 400 mm/h. Distribution of phases barely varied due to the inco...
| Autores: | , , , |
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| Formato: | artículo |
| Estado: | Versión publicada |
| Fecha de publicación: | 2020 |
| País: | España |
| Recursos: | Consejo Superior de Investigaciones Científicas (CSIC) |
| Repositorio: | DIGITAL.CSIC. Repositorio Institucional del CSIC |
| OAI Identifier: | oai:digital.csic.es:10261/219088 |
| Acesso em linha: | http://hdl.handle.net/10261/219088 |
| Access Level: | acceso abierto |
| Palavra-chave: | Nd2SiO5Nd9.33(SiO4)6O2 Raman spectroscopy Laser floating zone |
| Resumo: | Highly textured polycrystalline fibres of monoclinic P21/c Nd2SiO5 and hexagonal P63/m Nd9.33(SiO4)6O2 phases were obtained by Laser Floating Zone in air from stoichiometric mixtures of Nd2O3 and SiO2 changing the pulling rate from 10 to 400 mm/h. Distribution of phases barely varied due to the incongruent melt of the Nd2O3:SiO2 system, resulting in fibres adequate for microwave devices owing to the dielectric character of the Nd2SiO5 phase. Raman analysis was performed in this material for the first time. |
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