A sequential determination of Sr-90 and Po-210 in food samples

The latest EU Council Regulation 2016/52/Euratom updates the emergency limits on radionuclides in foods including 210Po and 90Sr, two of the most important radionuclides for radiological dose from the ingestion pathway. A novel and straightforward method has been developed for sequential determinati...

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Detalles Bibliográficos
Autores: Hurtado Bermúdez, Santiago José, Más Balbuena, José Luis, Villa Alfageme, María
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2017
País:España
Institución:Universidad de Sevilla (US)
Repositorio:idUS. Depósito de Investigación de la Universidad de Sevilla
OAI Identifier:oai:idus.us.es:11441/156879
Acceso en línea:https://hdl.handle.net/11441/156879
https://doi.org/10.1016/j.foodchem.2017.02.077
Access Level:acceso abierto
Palabra clave:210Po
90Sr
Sequential determination
LSC
Alpha-particle spectrometry
Seafood
Descripción
Sumario:The latest EU Council Regulation 2016/52/Euratom updates the emergency limits on radionuclides in foods including 210Po and 90Sr, two of the most important radionuclides for radiological dose from the ingestion pathway. A novel and straightforward method has been developed for sequential determination of 90Sr and 210Po in food samples using ultra low-level liquid scintillation counting and alpha-particle spectrometry. For 90Sr analysis, the method makes use of stable strontium as yield tracer, and 210Po is determined through self-deposition using 209Po as a yield tracer. The quantification limit for this method is 25.0 and 2.0 Bq kg−1 for 90Sr and 210Po, respectively. The proposed radiochemical separation can be completed within 2 days for a batch of 12 samples. The radiochemical procedure was validated by its application for the measurement of IAEA certified reference materials, and through participation in a national intercomparison exercise. Results are also presented in seafood from the Mediterranean coast.